Batman
Wealthy entrepreneur Bruce Wayne and his ward Dick Grayson lead a double life: they are actually crime fighting duo Batman and Robin. A secret Batpole in the Wayne mansion leads to the Batcave, where Police Commissioner Gordon often calls with the latest emergency threatening Gotham City. Racing to the scene of the crime in the Batmobile, Batman and Robin must (with the help of their trusty Bat-utility-belt) thwart the efforts of a variety of master criminals, including The Riddler, The Joker, Catwoman, and The Penguin.

Season 2 · Episode 46 ·
A Riddling Controversy
After two more robberies, the Riddler has enough money to purchase Professor Charm's Demolecularizer. He demonstrates his weapon on a park statue, then issues an ultimatum - if all criminal statutes are not rescinded within two hours, he will begin dissolving every building in Gotham City. He rigs his device to automatically fire on police headquarters if his demands are not met. The city's only hope is Batman, who believes he has a plan to counteract the device.
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Episode 46 of season 2 of Batman: “A Riddling Controversy”. Aired 1967-02-09. Watch it online free on ZapFlix.