Batman
Wealthy entrepreneur Bruce Wayne and his ward Dick Grayson lead a double life: they are actually crime fighting duo Batman and Robin. A secret Batpole in the Wayne mansion leads to the Batcave, where Police Commissioner Gordon often calls with the latest emergency threatening Gotham City. Racing to the scene of the crime in the Batmobile, Batman and Robin must (with the help of their trusty Bat-utility-belt) thwart the efforts of a variety of master criminals, including The Riddler, The Joker, Catwoman, and The Penguin.

Season 2 · Episode 55 ·
Black Widow Strikes Again
The Black Widow uses her cerebrum short-circuiting device to rob bank after bank in Gotham City. Batman and Robin soon catch up with her, but actually capturing the villainess proves harder than expected. Despite her nerve paralyzer spray, and two remote-control dummies that try to throw the Dynamic Duo off course, they finally make it inside the Black Widow's lair. But soon after entering, they are trapped in a giant web with two deadly black widow spiders.
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Episode 55 of season 2 of Batman: “Black Widow Strikes Again”. Aired 1967-03-15. Watch it online free on ZapFlix.